Analytical Chemistry
Topic outline
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This course will provide students with a basic understanding of analytical chemistry and major aspects of quantitative chemical analysis. The course is an introductory part of a series of analytical chemistry courses for industrial chemistry program. It will concentrate upon descriptive analytical chemistry and analytical methods based on chemical equilibrium which include precipitation and volumetric analysis.
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1.1 Analytical Methodology
1.2 Selection of Analytical Techniques
1.3 Concentration Units
1.4 Preparation of Solutions
1.5 Dilution
1.6 Chemical Stoichiometry-
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2.1 Measurement and Readings
2.2 Errors in Chemical Analysis
2.3 Graph and Measurement
2.4 Statistics to Data Evaluation
2.5 Uncertainty in Chemical Analysis
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3.1 Analytical Balance
3.2 Buoyancy
3.3 Volume Measurement
3.3.1 Burette
3.3.2 Volumetric Flask
3.3.3 Pipette
3.3.4 Syringe
3.4 Filtration
3.5 Drying
3.6 Calibration of Glassware
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4.1 Sampling
4.1.1 Homogenization of Samples
4.1.2 Sample Integrity
4.1.3 Physical Separation
4.1.4 Types of Sample
4.1.5 Types of Sample Matrices
4.2 Sample Preparation
4.2.1 Percentage Recovery
4.2.2 Optimization of Chemical Form
4.2.3 Separation and Preconcentration Techniques
4.2.4 Dissolution
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5.1 Response Factor
5.2 Peak Area Measurement Methods
5.2.1 Percent Composition
5.2.2 Corrected Percent Peak Area
5.3 Quantitation
5.3.1 External Standard Calibration
5.3.2 Internal Standard Calibration
5.3.3 Standard Addition Method
5.4 Calibration Method
5.5 Linear Regression
5.6 Noise
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6.1 Equilibrium
6.2 Le Chateliar's Principles
6.3 Introduction to Titration
6.4 Types of Titrimetry
6.5 Titrant and Titrand
6.6 Volumetric Calculations
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7.1 Terms Used in Titrimetry
7.2 Desirable Properties of Standard Solutions
7.3 Volumetric Calculations
7.4 Overview of Gravimetry
7.5 Precipitation Gravimetry
7.6 Volatization Gravimetry
7.7 Particulate Gravimetry
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8.1 Solutions and Indicator for Acid/Base Titrations
8.2 Titration of Strong Acids and Strong Bases
8.3 Titration Curves for Weak Acids
8.4 Titration Curves for Weak Bases
8.5 The Composition of Solutions During Acids/Bases Titration
8.6 Buffer Solutions
8.7 Application of Neutralization Titrations
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9.1 Introduction to Precipitation Titration
9.2 Methods in Precipitation Titration
9.2.1 Mohr's Method
9.2.2 Fajan's Method
9.2.3 Volhard Method
9.3 Limitation of Precipitation Titration
9.4 Applications of Precipitation Titration
9.5 Precipitation Titration Curve Involving Silver Ion
9.5.1 Applications of Standard Silver Nitrate Solutions
9.5.2 Calculating the Titration Curve
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10.1 Introduction Complexometric Titration
10.2 Titration with Inorganic Complexing Agents
10.3 Organic Complexing Agents
10.4 Aminocarboxylic Acid Titrations
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11.1 Oxidation-Reduction Reaction
11.2 Redox Titration Curve
11.3 Redox Indicator
11.4 Applications of Redox Titration